Trimethyl(3,5-xylyloxy)silane synthesis
- Product Name:Trimethyl(3,5-xylyloxy)silane
- CAS Number:17994-05-7
- Molecular formula:
- Molecular Weight:0
108-38-3
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Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: 2-(t-butylazo)prop-2-yl hydroperoxide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / benzene / 44.84 °C
1.2: 2 h / 75 °C / Inert atmosphere
2.1: triethylamine / dichloromethane / 0.17 h / Inert atmosphere
2.2: 20 °C / Inert atmosphere
References:
Moores, Lee C.;Kaur, Devinder;Smith, Mathew D.;Poole, James S. [Journal of Organic Chemistry,2019,vol. 84,# 6,p. 3260 - 3269]
