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ChemicalBook CAS DataBase List Trimethyl orthobenzoate
707-07-3

Trimethyl orthobenzoate synthesis

12synthesis methods
The phenylbenzamide derivative (44.3 mmol) and methyl trifluoromethanesulfonate (5.93 mL, 52.5 mmol) were dissolved in dry dichloromethane (20 mL) and the reaction solution was stirred for 18 hours. Anhydrous ether (70 mL) was added to the reaction mixtur
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: hydrogenchloride / 10 h / 5 - 10 °C
2: 240 h / 20 °C

References:

Noe, Marco;Perosa, Alvise;Selva, Maurizio [Green Chemistry,2013,vol. 15,# 8,p. 2252 - 2260]

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