TRIMETHYLSILYLBENZENESULFONATE synthesis
- Product Name:TRIMETHYLSILYLBENZENESULFONATE
- CAS Number:17882-06-3
- Molecular formula:C9H14O3SSi
- Molecular Weight:230.36
14468-90-7
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515-46-8
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$25.00/5g
2687-91-4
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$6.00/25g
17882-06-3
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Yield: 59% ， 72%
Reaction Conditions:
Heating;
Steps:
Synthesis of N-alkyl-substituted derivatives 4a-h
General procedure: A mixture of alkyl sulfonate 1 (0.05-0.1 mol) with equimolar amount of N-silyl derivative of 2 was heated for 3-5 h at 140-170 °C, then fractioned.
References:
Baukov, Yu. I.;Kramarova, E. P.;Negrebetsky, Vad. V.;Shagina, A. D.;Shipov, A. G.;Tarasenko, D. V. [Russian Chemical Bulletin,2020,vol. 69,# 2,p. 398 - 400][Izv. Akad. Nauk, Ser. Khim.,2020,vol. 69,# 2,p. 398 - 400,3]
768-32-1
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$10.00/500mg
17882-06-3
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515-46-8
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$25.00/5g
7449-74-3
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$15.00/5g
38806-26-7
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$409.00/1g
17882-06-3
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515-46-8
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$25.00/5g
3553-94-4
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19797-08-1
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17882-06-3
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515-46-8
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$25.00/5g
10557-63-8
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529-65-7
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$435.00/1000g
17882-06-3
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