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ChemicalBook CAS DataBase List TRIS-(4-AMINOPHENYL)THIOPHOSPHATE
52664-35-4

TRIS-(4-AMINOPHENYL)THIOPHOSPHATE synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 4 steps
1: tetrahydrofuran / 30 h
2: triethylamine; phosphorus trichloride / toluene / 24 h / 0 - 20 °C / Inert atmosphere
3: sulfur / 30 h / Inert atmosphere; Reflux
4: trifluoroacetic acid / dichloromethane / 4 h

References:

Butler, Patrick W. V.;Kruger, Paul E.;Ward, Jas S. [Chemical Communications,2019,vol. 55,# 69,p. 10304 - 10307]

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