METHYL-D3 ACETATE synthesis
- Product Name:METHYL-D3 ACETATE
- CAS Number:24704-57-2
- Molecular formula:C3H3D3O2
- Molecular Weight:77.1
811-98-3
225 suppliers
$18.69/1g
141-78-6
723 suppliers
$22.37/250ml
925-93-9
94 suppliers
$58.50/25ml
24704-57-2
13 suppliers
$502.62/5MG
Yield:-
Reaction Conditions:
with N-ethyl-N,N-diisopropylamine at 21.5;Kinetics;
Steps:
7
General procedure: For each kinetics trial, 1.00 mL of a 1.03 M (i-Pr)2NEt/MeOH-d4 solution was added to a measured amount of ester so that the initial concentration of ester was about 0.1 M. Kinetics data were collected as a series of signal integrations with a Bruker Avance DPX-300 NMR spectrometer. Each rate constant was calculated by the least-squares method for the simple linear regression equation ln (%ROAc) = -kt + C. Each value in Table 2 is the average of at least two determinations.
References:
Hankins, Jamilah N.;Gouws, Michele;Mahajer, Amir;Kim, Ethan S.;Gwaltney, Kevin P.;Haseltine, John [Tetrahedron Letters,2012,vol. 53,# 19,p. 2450 - 2453] Location in patent:experimental part
811-98-3
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$18.69/1g
75-36-5
576 suppliers
$17.92/100G
24704-57-2
13 suppliers
$502.62/5MG
811-98-3
225 suppliers
$18.69/1g
64-19-7
1679 suppliers
$10.00/25ML
79-20-9
589 suppliers
$14.00/100g
24704-57-2
13 suppliers
$502.62/5MG
811-98-3
225 suppliers
$18.69/1g
122-79-2
263 suppliers
$14.00/1g
79-20-9
589 suppliers
$14.00/100g
24704-57-2
13 suppliers
$502.62/5MG
108-95-2
778 suppliers
$14.00/25g