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ChemicalBook CAS DataBase List Glyoxylic acid monohydrate
563-96-2

Glyoxylic acid monohydrate synthesis

3synthesis methods
Using maleic anhydride as a raw material, a 20-40% maleic acid solution is obtained by hydrolysis. Ozone is introduced in series at 15-25°C for oxidation, with a molar ratio of ozone to maleic acid of approximately 1.2-1.25:1. The reaction solution is then subjected to vacuum distillation to recover formic acid and water, yielding an 80% glyoxylic acid solution. Finally, granular white glyoxylic acid monohydrate is obtained by crystallization.
-

Yield:-

Reaction Conditions:

at 25;Kinetics;in wss. Loesungen vom pH 8.27 bis pH 9.97;

References:

Kuta [Collection of Czechoslovak Chemical Communications,1959,vol. 24,p. 2532,2539, 2541] Soerensen et al. [Acta chemica Scandinavica. Series A: Physical and inorganic chemistry,1974,vol. 28,p. 162,167]

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