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ChemicalBook CAS DataBase List Citric acid monohydrate
5949-29-1

Citric acid monohydrate synthesis

1synthesis methods
Citric acid occurs naturally in a number of plant species and may be extracted from lemon juice, which contains 5–8% citric acid, or pineapple waste. Anhydrous citric acid may also be produced industrially by mycological fermentation of crude sugar solutions such as molasses, using strains of Aspergillus niger . Citric acid is purified by recrystallization; the anhydrous form is obtained from a hot concentrated aqueous solution and the monohydrate from a cold concentrated aqueous solution.
-

Yield:-

Reaction Conditions:

with sodium hydroxide

Steps:

Sample 14

Sample 14
An aqueous composition was prepared as follows. 1 g (4.8 mmol) of citric acid monohydrate (obtained from Jungbunzlauer) was added to a beaker and neutralized to a pH of 7.4 by addition of 1.2 g (15 mmol) of the 50% sodium hydroxide solution.
Next, 9 g (24.88 mmol) of the 25% sodium chlorite solution, 90 ml of deionized water, and 1 g (6.02 mmol) of the potassium iodide were added to the beaker, and the contents of the beaker were stirred in order to produce the aqueous composition.
The pH of the contents of the beaker was 11.7 while stirring.
At 120 days after the date of preparation of the composition, the pH of the composition was 9.1.

References:

US2018/179058,2018,A1

Citric acid monohydrate Related Search:

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