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ChemicalBook >> journal list >> Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy >>article

Spectroscopic and biological approach of Ni(II) and Cu(II) complexes of 2-pyridinecarboxaldehyde thiosemicarbazone

Published:1 March 2008 DOI: 10.1016/j.saa.2007.05.033 PMID: 17627876
Sulekh Chandra , Smriti Raizada , Monika Tyagi , Praveen Kumar Sharma

Abstract

Ni(II) and Cu(II) complexes having the general composition [M(L)2X2] [where L?=?2-pyridinecarboxaldehyde thiosemicarbazone, M?=?Ni(II) and Cu(II), X?=?Cl?, NO3? and 1/2 SO42?] have been synthesized. All the metal complexes were characterized by elemental analysis, molar conductance, magnetic moment, mass, IR, EPR and electronic spectral studies. The magnetic moment measurements of the complexes indicate that all the complexes are of high-spin type. On the basis of spectral studies an octahedral geometry has been assigned for Ni(II) complexes whereas tetragonal geometry for Cu(II) except [Cu(L)2SO4] which posseses five coordinated geometry. The ligand and its metal complexes were screened against phytopathogenic fungi and bacteria in vitro.

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