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The Journal of Organic Chemistry

The Journal of Organic Chemistry

IF: 3.3
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Fluorination of Thiocarbonyl Compounds with Bis(2-methoxyethyl)aminosulfur Trifluoride (Deoxo-Fluor Reagent):? A Facile Synthesis of gem-Difluorides

Published:11 July 2000 DOI: 10.1021/jo000020j PMID: 10956459
Gauri S. Lal, Elyse Lobach, Ann Evans

Abstract

A variety of thiocarbonyl derivatives (thioketone, thioester, thioamide, dithioester, and dithiocarbamate) were converted to the corresponding gem-difluorides in excellent yields on reaction with the fluorinating agent, bis(2-methoxyethyl)aminosulfur trifluoride, in the presence of SbCl3.

Substances (2)

Related products
Procduct Name CAS Molecular Formula Supplier Price
Antimony trichloride 10025-91-9 Cl3Sb 263 suppliers $10.00-$1152.35
Bis(2-methoxyethyl)aminosulfur trifluoride 202289-38-1 C6H14F3NO2S 254 suppliers $24.00-$8800.00

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