1-Amino-2-naphthol synthesis
- Product Name:1-Amino-2-naphthol
- CAS Number:2834-92-6
- Molecular formula:C10H9NO
- Molecular Weight:159.18
550-60-7
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$45.00/50mg
2834-92-6
103 suppliers
$200.00/500 mg
Yield:2834-92-6 99%
Reaction Conditions:
with hydrogen in water at 20 - 50; for 1 h;Temperature;
Steps:
2.1; 2.2 2) Catalytic hydrogenation reaction Add
82.5g of the prepared 1-nitroso-2-naphthol to 825.0g of water, stir at room temperature until dissolved, and simultaneously open the pump C and hydrogen pressure reducing valve, pump C (flow rate is 15mL/min), Hydrogen gas flows into the tubular reactor after the pressure reducing valve. The tubular reactor is placed at 50°C with a residence time of 1h. The reaction liquid flows into the receiving bottle, and then it is rotovaped until the solution is saturated. It precipitates in ice water and is filtered to obtain white crystals. 73.1g, the yield was 99%, and its content measured by HPLC was 96.8%.
References:
Zhejiang University of Technology;Yu Zhiqun;Huang Jiajia;Xie Shitian;Su Weike CN111217764, 2020, A Location in patent:Paragraph 0011; 0032; 0035-0036; 0041; 0044-0045
135-19-3
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$9.00/1g
2834-92-6
103 suppliers
$200.00/500 mg
131-91-9
274 suppliers
$6.00/1g
2834-92-6
103 suppliers
$200.00/500 mg
842-07-9
458 suppliers
$21.00/25g
2834-92-6
103 suppliers
$200.00/500 mg
62-53-3
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$10.00/1g
13082-06-9
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2834-92-6
103 suppliers
$200.00/500 mg