1-BOC-2,2-DIMETHYL-PIPERAZINE synthesis
- Product Name:1-BOC-2,2-DIMETHYL-PIPERAZINE
- CAS Number:674792-07-5
- Molecular formula:C11H22N2O2
- Molecular Weight:214.3
84477-72-5
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674792-07-5
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: triethylamine / dichloromethane / 3 h / -78 - 20 °C
2: triethylamine / dichloromethane / 18 h / Inert atmosphere
3: palladium 10% on activated carbon; hydrogen / ethyl acetate / 5 h
References:
CALIFORNIA INSTITUTE OF TECHNOLOGY;THE REGENTS OF THE UNIVERSITY OF CALIFORNIA;1200 PHARMA LLC;O'BOYLE, Brendan, M.;HILF, Justin, A.;VIRGIL, Scott, C.;SUN, Alexander, W.;STOLTZ, Brian, M.;CONKLIN, Dylan;MCDERMOTT, Martina;O'BRIEN, Neil, A.;PALAZZOLO, Michael, J.;SLAMON, Dennis;BARTBERGER, Michael, D. WO2020/23917, 2020, A1