2-(1,3-dioxolan-2-yl)Benzaldehyde synthesis
- Product Name:2-(1,3-dioxolan-2-yl)Benzaldehyde
- CAS Number:59259-01-7
- Molecular formula:C10H10O3
- Molecular Weight:178.18
6630-33-7
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Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: toluene-4-sulfonic acid / toluene / 18 h / Reflux; Inert atmosphere
2.1: n-butyllithium / tetrahydrofuran / -78 - -30 °C / Inert atmosphere
2.2: -78 - 20 °C / Inert atmosphere
References:
Che, Chao;Li, Song;Yu, Zhixiong;Li, Fangfang;Xin, Shengchang;Zhou, Liyan;Lin, Shuo;Yang, Zhen [ACS Combinatorial Science,2013,vol. 15,# 4,p. 202 - 207]
23691-82-9
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1708-41-4
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107-02-8
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$38.60/4s8501
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68348-23-2
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