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ChemicalBook CAS DataBase List 3,5,5-Trimethylhexanoyl chloride
36727-29-4

3,5,5-Trimethylhexanoyl chloride synthesis

2synthesis methods
Isononanoic acid (300 g, 1 eq.) was added to a 500 mL reaction vial, and phosgene (1-5 eq.) was introduced at a constant rate at a certain temperature, and the reaction was monitored by gas chromatography. At the end of the reaction, dry nitrogen was intr
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: air; magnesium acetate; glacial acetic acid / 25 °C
2: SOCl2

References:

Bruner [Industrial and Engineering Chemistry,1949,vol. 41,p. 2861]

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