3,5-Difluorobenzoic acid synthesis
- Product Name:3,5-Difluorobenzoic acid
- CAS Number:455-40-3
- Molecular formula:C7H4F2O2
- Molecular Weight:158.1
32085-88-4
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$19.00/25g
455-40-3
326 suppliers
$10.00/5g
Yield:455-40-3 78%
Reaction Conditions:
with diphenyl diselenide;dihydrogen peroxide in water at 20; for 6 h;Green chemistry;
Steps:
3.2. General Procedure for the Synthesis of Carboxylic Acids 2
General procedure: Diphenyl diselenide (3, 0.006 g; 0.02 mmol) was treated with H2O2 (30%·w/w, 0.1 mL, 1 mmol) andwater (0.2 mL) and stirred at room temperature at 800 rpm until the discoloration of the reaction mixture;then, the aldehyde 1 (1 mmol) was added. After 6 h, the aqueous mixture was extracted three times withEtOAc (3 × 20 mL). The collected organic layers were dried over Na2SO4 and the solvent evaporatedunder reduced pressure.
References:
Sancineto, Luca;Tidei, Caterina;Bagnoli, Luana;Marini, Francesca;Lenardo, Eder J.;Santi, Claudio [Molecules,2015,vol. 20,# 6,p. 10496 - 10510]
124-38-9
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$175.00/23402
461-96-1
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$6.00/10g
455-40-3
326 suppliers
$10.00/5g
124-38-9
724 suppliers
$175.00/23402
2713-34-0
417 suppliers
$5.00/1g
455-40-3
326 suppliers
$10.00/5g
124-38-9
724 suppliers
$175.00/23402
651027-07-5
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455-40-3
326 suppliers
$10.00/5g