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ChemicalBook CAS DataBase List 3-ethoxy-5-iodo-4-methoxybenzaldehyde
428483-80-1

3-ethoxy-5-iodo-4-methoxybenzaldehyde synthesis

2synthesis methods
54246-05-8 Synthesis
3,4-dihydroxy-5-iodobenzaldehyde

54246-05-8
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3-ethoxy-5-iodo-4-methoxybenzaldehyde

428483-80-1
9 suppliers
inquiry

-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 0.83 h / 20 °C / Inert atmosphere
1.2: 5 h / 20 °C / Inert atmosphere
2.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 0.58 h / 20 °C / Inert atmosphere
2.2: 0.5 h / 20 °C / Inert atmosphere

References:

Nammalwar, Baskar;Bunce, Richard A.;Berlin, K. Darrell;Bourne, Christina R.;Bourne, Philip C.;Barrow, Esther W.;Barrow, William W. [Organic Preparations and Procedures International,2012,vol. 44,# 2,p. 146 - 152]

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