4-Isopropylbenzoic acid synthesis
- Product Name:4-Isopropylbenzoic acid
- CAS Number:536-66-3
- Molecular formula:C10H12O2
- Molecular Weight:164.2
536-60-7
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$25.00/25mL
536-66-3
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$5.00/5g
Yield:536-66-3 98%
Reaction Conditions:
with diethylene glycol dimethyl ether at 70; for 0.5 h;Sonication;
Steps:
15 Example 15: Preparation of 4-isopropylbenzoic acid:
In a 10 mL round bottom flask, 0.75 g of 4-isopropylbenzyl alcohol was added in sequence.2 g of diethylene glycol dimethyl ether, the resulting mixture was subjected to ultrasonic irradiation at 40 KHz/30 W/70 ° C for 30 minutes in an ultrasonic reaction apparatus. The diethylene glycol dimethyl ether was removed under reduced pressure and recrystallized to give 0.79 g of 4-isopropylbenzoic acid, yield 98%.
References:
CN108467342,2018,A Location in patent:Paragraph 0126; 0127
99-87-6
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536-66-3
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$5.00/5g
645-13-6
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$11.00/5g
536-66-3
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$5.00/5g
100-21-0
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586-89-0
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$10.00/1g