6-Chlorohex-1-ene synthesis
- Product Name:6-Chlorohex-1-ene
- CAS Number:928-89-2
- Molecular formula:C6H11Cl
- Molecular Weight:118.6
105-53-3
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Yield: 81%
Reaction Conditions:
with sodium in ethanol
Steps:
S.2.2 2)
To 1000 ml of absolute ethanol was added 4 g (0.174 mole) of sodium, and 20 g (0.125 mole) of diethyl malonate was then added thereto. Further, 14 g (0.118 mole) of 5-hexenyl chloride as obtained in (1) above was slowly added thereto, followed by refluxing for 2 hours. The reaction mixture was freed of the solvent by distillation, and the residue was distilled to obtain 23.2 g (yield: 81%) of diethyl 5-hexenylmalonate having a boiling point of 115°-116° C./3 mmHg.
References:
Takasago International Corporation US5141921, 1992, A
10297-06-0
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18922-06-0
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2622-05-1
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109-70-6
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10297-06-0
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544-10-5
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928-89-2
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