7-Methylindole synthesis
- Product Name:7-Methylindole
- CAS Number:933-67-5
- Molecular formula:C9H9N
- Molecular Weight:131.17
136-80-1
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$222.00/1g
933-67-5
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$6.00/1g
Yield:933-67-5 64.3%
Reaction Conditions:
with o-toluidine in acetonitrile
Steps:
8 Example 8
This embodiment provides a quinone compound, and its reaction formula is:In a reaction flask, 5 mmol of N-hydroxyethyl-2-methylaniline and 7.5 mmol of 2-methylaniline provided in Example 2 were weighed out and dissolved in 200 ml of acetonitrile, and Sn/activated carbon loaded catalyst was added, and TLC was used to detect N. The reaction was stopped after the reaction of hydroxyethyl-2-methylaniline was completed.After isolation and purification, 7-methylindole was obtained (yield 64.3%).
References:
Chongqing Huage Biochemical Co., Ltd.;He Xiaoqiang;Chen Zhizhong;Wu Chengli CN107445881, 2017, A Location in patent:Paragraph 0065-0069
65673-86-1
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933-67-5
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107-21-1
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95-53-4
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933-67-5
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$6.00/1g
136-80-1
57 suppliers
$222.00/1g
94-92-8
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$50.10/5g
3367-47-3
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