o-Toluidine synthesis
- Product Name:o-Toluidine
- CAS Number:95-53-4
- Molecular formula:C7H9N
- Molecular Weight:107.15
31656-92-5
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$229.00/10ml
95-53-4
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$10.00/1g
Yield:95-53-4 93%
Reaction Conditions:
with 2-(bis(4-methoxyphenyl)phosphanyl)-5-methylbenzenesulfonamide in tetrahydrofuran at 30; for 3 h;Inert atmosphere;Staudinger Azide Reduction;
Steps:
General Procedure A (for the substrates 1a-1m)
General procedure: Under a N2 atmosphere, the correspondingorganic azide (1.00 mmol, 1.0 equiv) was dissolved in anhydrous tetrahydrofuran(10 mL), followed by the addition of 2c (1.10 mmol, 1.1 equiv). The mixture was stirredat 30 C for 3 h. Upon completion, the mixture was concentrated in vacuo and the crudeproduct was purified by flash column chromatography.
References:
Li, Xingzhuo;Wang, Zhenguo;Luo, Wenjun;Wang, Zixu;Yin, Keshu;Li, Le [Molecules,2022,vol. 27,# 17,art. no. 5707]
16419-60-6
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95-53-4
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$10.00/1g
95-46-5
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95-53-4
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88-72-2
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$15.00/5g
95-53-4
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$10.00/1g
615-37-2
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$5.00/5g
95-53-4
462 suppliers
$10.00/1g