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ChemicalBook CAS DataBase List [1,1'-Bis(diphenylphosphino)ferrocene]dichloropalladium(II)
72287-26-4

[1,1'-Bis(diphenylphosphino)ferrocene]dichloropalladium(II) synthesis

1synthesis methods

A method for the preparation of 1,1'-bis(diphenylphosphino)ferrocene palladium dichloride II (dppfPdCl2) comprising the steps of:

(a) adding palladium chloride to concentrated hydrochloric acid, heating to 40-80°C to dissolve, the amount of

12150-46-8 Synthesis
1,1'-Bis(diphenylphosphino)ferrocene

12150-46-8
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Palladium, bis(acetonitrile)dichloro-, (SP-4-2)-

90243-59-7
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Yield:72287-26-4 97%

Reaction Conditions:

in benzene;stirred at room temp. for 12 h; ppt. filtered, washed with benzene, dried in vac., recrystn. (CHCl3); elem. anal.;

References:

Hayashi, Tamio;Konishi, Mitsuo;Kobori, Yuji;Kumada, Makoto;Higuchi, Taiichi;Hirotsu, Ken [Journal of the American Chemical Society,1984,vol. 106,p. 158 - 163]

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