AKOS 93602 synthesis
- Product Name:AKOS 93602
- CAS Number:40017-83-2
- Molecular formula:C9H6N2O3
- Molecular Weight:190.16
Yield:40017-83-2 69%
Reaction Conditions:
Stage #1: acetonitrilewith n-butyllithium in tetrahydrofuran;hexane at -78; for 1 h;Sealed tube;Inert atmosphere;
Stage #2: methyl 2-nitrobenzoate in tetrahydrofuran;hexane at -45; for 3.25 h;Sealed tube;Inert atmosphere;
References:
Lee, Seok Beom;Jang, Yoonkyung;Ahn, Jiwon;Chun, Simin;Oh, Dong-Chan;Hong, Suckchang [Organic Letters,2020,vol. 22,# 21,p. 8382 - 8386] Location in patent:supporting information
141342-35-0
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40017-83-2
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610-14-0
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$61.89/5g
40017-83-2
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91974-26-4
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40017-83-2
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