Benzyldimethylhexadecylammonium chloride synthesis
- Product Name:Benzyldimethylhexadecylammonium chloride
- CAS Number:122-18-9
- Molecular formula:C25H46ClN
- Molecular Weight:396.09
112-69-6
282 suppliers
$9.00/25g
100-44-7
644 suppliers
$13.50/250G
122-18-9
356 suppliers
$8.00/10g
Yield:122-18-9 92.1%
Reaction Conditions:
in ethanol at 40; for 6 h;Large scale;Solvent;Temperature;
Steps:
2; 8-9 Example 3 Preparation of Cetyl Dimethylbenzyl Ammonium Chloride
Into a 50 L reactor, 6.00 kg (22.3 mol) of cetyldimethylamine, 2.82 kg (22.3 mol) of benzyl chloride and 18.00 kg of ethanol were added, and the mixture was stirred at 40 ° C for 6 h. Then cool down to -5 °C. After the solid is precipitated, it is filtered.Drying gave 8.12 kg of a white solid with a total yield of 92.1%. The purity of cetyldimethylbenzylammonium chloride was 99.4%.
References:
Hubei Gedian Ren Fu Yaoyong Fuliao Co., Ltd.;Zhang Yangyang;Tian Jia;Cao Jin;Ran Wenhua;Li Sheng CN109553539, 2019, A Location in patent:Paragraph 0035-0036; 0045-0048
36653-82-4
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$6.00/100g
122-18-9
356 suppliers
$8.00/10g
4860-03-1
286 suppliers
$6.00/25g
122-18-9
356 suppliers
$8.00/10g
