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ChemicalBook CAS DataBase List Chloromethanesulfonyl chloride
3518-65-8

Chloromethanesulfonyl chloride synthesis

11synthesis methods

Chloromethylsulfonyl chloride is synthesized as follows: add Na2SO3252g, 500g of water, 504g of methylene chloride, I1.25g of cetyltrimethylammonium chloride to 2000ml of the reactor with a pressure and temperature detecting device, warm up to 0.2MPa p

-

Yield:3518-65-8 62%

Reaction Conditions:

with potassium chlorate in hydrogenchloride for 5 h;Ambient temperature;

References:

Fares, Fares A.;Ridley, Damon D.;Yin, Ping [Australian Journal of Chemistry,1997,vol. 50,# 10,p. 1027 - 1029]

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