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ChemicalBook CAS DataBase List Cytosine
71-30-7

Cytosine synthesis

14synthesis methods
-

Yield:71-30-7 93%

Reaction Conditions:

with dihydrogen peroxide at 80; for 20 h;Temperature;

Steps:

5

30% hydrogen peroxide (51.0 g, 0.45 mol) was added dropwise to the intermediate solution, drop finished, heating up to 80 ° C for 20 hours; cooled to room temperature, dropping 10mol / L sodium hydroxide solution to adjust the pH value, when the pH is 7.5, continue to cool to 10 ° C; after cooling, washed, after drying to obtain cytosine 31.0g, The yield was 93.0% and the HPLC content was 99.4%.

References:

CN103880758,2016,B Location in patent:Paragraph 0019

Cytosine Related Search:

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