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(DIETHOXYPHOSPHORYL)DIFLUOROACETIC ACID synthesis

1synthesis methods

1478-53-1 Synthesis

Yield:97480-37-0 69%

Reaction Conditions:

with lithium diisopropyl amide in tetrahydrofuran;1.) -78 deg C, 30 min, 2.) -78 to 0 deg C;

References:

Hamilton, Chris J.;Roberts, Stanley M. [Journal of the Chemical Society. Perkin transactions I,1999,# 8,p. 1051 - 1056]

DIFLUOROMETHYLPHOSPHONIC ACID DIETHYL ESTER Difluoroacetic acid Triethyl 2-fluoro-2-phosphonoacetate

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