一二三四区视频,亚洲少妇熟女色,日本久热无码视频网,欧美国产日韩大尺度,亚洲a视频,久久少妇一区二区,日韩999无码视频,刺激久久久久久久,啊啊啊啊不要啊在线

Welcome to chemicalbook!
Chinese English Japanese Germany Korea
010-86108875
Try our best to find the right business for you.
Do not miss inquiry messages Please log in to view all inquiry messages.

Welcome back!

ChemicalBook CAS DataBase List Ethyl caprate
110-38-3

Ethyl caprate synthesis

11synthesis methods
By esterification of decanoic acid and ethyl alcohol in the presence of HCl or H2SO4.
-

Yield:110-38-3 97%

Reaction Conditions:

with alumina methanesulfonic acid at 120; for 0.333333 h;Microwave irradiation;

Steps:

Representative Procedure for Preparation of Aromatic and Aliphatic Esters (Table 1)
General procedure: In a typical reaction, AMA 2:3 (332 g, 0.6 mol), the corresponding carboxylicacid (1 mol), and alcohol (1.5-2 mol) were mixed in the provided reaction glass tubeequipped with a screw cap and magnetic agitation until a wet mixture was achieved.The reaction mixture was irradiated with microwaves (Anton Parr Monowave 300reactor) at 80 C for 8 min or 120 C for 20 min. On cooling, the mixture was diluted with dichloromethane (41 mL), filtered under gravity, and washed with dichloromethane;then the filtrate was washed with Na2CO3 (ss) and water. The organic layerwas dried over Na2SO4, filtered, and concentrated under reduced pressure to give theester.

References:

Fabian, Lucas;Gomez, Matias;Kuran, Juan A. Caturelli;Moltrasio, Graciela;Moglioni, Albertina [Synthetic Communications,2014,vol. 44,# 16,p. 2386 - 2392]

FullText

Ethyl caprate Related Search:

辽源市| 丹棱县| 射洪县| 宣化县| 宣城市| 新野县| 铜川市| 登封市| 定南县| 苏尼特右旗| 乌兰县| 德阳市| 四子王旗| 西城区| 南江县| 怀宁县| 安吉县| 咸阳市| 闽侯县| 伊宁县| 苏州市| 保山市| 布尔津县| 汉寿县| 乃东县| 阿坝| 连江县| 萍乡市| 赤壁市| 宁南县| 礼泉县| 安乡县| 栾川县| 灯塔市| 海兴县| 波密县| 南宁市| 寿光市| 临猗县| 云浮市| 通辽市|