Ethyl phenylacetate synthesis
- Product Name:Ethyl phenylacetate
- CAS Number:101-97-3
- Molecular formula:C10H12O2
- Molecular Weight:164.2
103-79-7
0 suppliers
$28.00/10mg
105-58-8
484 suppliers
$15.00/25g
101-97-3
481 suppliers
$14.00/25mL
Yield:101-97-3 100%
Reaction Conditions:
with Novozym 435;acylase I from Aspergillus melleus;amano lipase AK from pseudomonas fluorescens;lipase from wheat germ;papaine in toluene at 40; for 48 h;Mechanism;Enzymatic reaction;
Steps:
4.3. Experimental setup
General procedure: To the solution of acid (1 mmol) in toluene (1 ml), the corresponding dialkyl carbonate (2 mmol) and enzymes (per 4 mg of each enzyme) were added in 5 ml vial. The reaction mixture was stirring for 24 or 48 h at 40 °C in vortex mixture (Heidolph Promax 1020) equipped with incubator (Heidolph Inkubator 1000). After cooling, the mixture was washed with NaHCO3 (3×) and brine (1×). Organic solvent was removed under vacuum to obtain the product 2a-2r.
References:
Zysk, Malgorzata;Zadlo, Anna;Brodzka, Anna;Wisniewska, Catalina;Ostaszewski, Ryszard [Journal of Molecular Catalysis B: Enzymatic,2014,vol. 102,p. 225 - 229]
64-17-5
857 suppliers
$10.00/50g
201230-82-2
1 suppliers
inquiry
100-44-7
642 suppliers
$13.50/250G
101-97-3
481 suppliers
$14.00/25mL
64-17-5
857 suppliers
$10.00/50g
103-81-1
358 suppliers
$13.00/5g
101-97-3
481 suppliers
$14.00/25mL
103-82-2
0 suppliers
$22.60/100g
64-17-5
857 suppliers
$10.00/50g
101-97-3
481 suppliers
$14.00/25mL
591-50-4
500 suppliers
$10.00/1g
141-97-9
859 suppliers
$5.00/25g
101-97-3
481 suppliers
$14.00/25mL