Ethyl phenylacetate synthesis
- Product Name:Ethyl phenylacetate
- CAS Number:101-97-3
- Molecular formula:C10H12O2
- Molecular Weight:164.2
103-79-7
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$28.00/10mg
105-58-8
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$15.00/25g
101-97-3
485 suppliers
$14.00/25mL
Yield:101-97-3 100%
Reaction Conditions:
with Novozym 435;acylase I from Aspergillus melleus;amano lipase AK from pseudomonas fluorescens;lipase from wheat germ;papaine in toluene at 40; for 48 h;Mechanism;Enzymatic reaction;
Steps:
4.3. Experimental setup
General procedure: To the solution of acid (1 mmol) in toluene (1 ml), the corresponding dialkyl carbonate (2 mmol) and enzymes (per 4 mg of each enzyme) were added in 5 ml vial. The reaction mixture was stirring for 24 or 48 h at 40 °C in vortex mixture (Heidolph Promax 1020) equipped with incubator (Heidolph Inkubator 1000). After cooling, the mixture was washed with NaHCO3 (3×) and brine (1×). Organic solvent was removed under vacuum to obtain the product 2a-2r.
References:
Zysk, Malgorzata;Zadlo, Anna;Brodzka, Anna;Wisniewska, Catalina;Ostaszewski, Ryszard [Journal of Molecular Catalysis B: Enzymatic,2014,vol. 102,p. 225 - 229]
64-17-5
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201230-82-2
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100-44-7
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101-97-3
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$14.00/25mL
64-17-5
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103-81-1
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101-97-3
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$14.00/25mL
103-82-2
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64-17-5
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$10.00/50g
101-97-3
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$14.00/25mL
591-50-4
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141-97-9
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101-97-3
485 suppliers
$14.00/25mL