Heptanoic acid synthesis
- Product Name:Heptanoic acid
- CAS Number:111-14-8
- Molecular formula:C7H14O2
- Molecular Weight:130.18
111-70-6
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111-14-8
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Yield:111-14-8 100%
Reaction Conditions:
with oxygen;potassium carbonate in lithium hydroxide monohydrate at 50; for 24 h;Green chemistry;
Steps:
2.5. Oxidation of benzyl alcohol catalysed by AuNPs/mf-MWCNT
General procedure: AuNPs/mf-MWCNT (3 mg, 1.88 mmol Au/g catalyst) in distilledwater (2 mL) was dispersed for 5 min by ultrasound. K2CO3 (0.08 g,0.6 mmol) and benzyl alcohol (20 mL, 0.2 mmol) was added into thereaction mixture and the mixturewas stirred under an atmosphericof oxygen for 16 h at 50 °C. The catalyst were collected by externalmagnet and washed three times with deionized water. The solution was neutralized with 0.1M HCl (pH = 3-4) and extracted withAcOEt (3 x 7 mL). The extracted organic layer was dried overNa2SO4 and then analyzed by gas chromatography. The GC yieldwas obtained from the calibration curve.
References:
Kaboudin, Babak;Saghatchi, Fatemeh;Kazemi, Foad [Journal of Organometallic Chemistry,2019,vol. 882,p. 64 - 69]
629-05-0
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111-14-8
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108-11-2
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111-14-8
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74299-84-6
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111-14-8
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111-66-0
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111-14-8
439 suppliers
$14.00/25G