Phosphorus tribromide synthesis
- Product Name:Phosphorus tribromide
- CAS Number:7789-60-8
- Molecular formula:Br3P
- Molecular Weight:270.69
Yield:7789-60-8 42%
Reaction Conditions:
in neat (no solvent);byproducts: Et4NIBr2; argon atmosphere; org. compd. addn. to PBr5 (cooling to -20°C), reaction vessel connecting to vac. line; PBr3 collection (trap cooled with liq. nitrogen);
References:
Vengel'nikova, V. N.;Timokhin, B. V.;Kalabina, A. V.;Donskikh, V. I. [Journal of general chemistry of the USSR,1982,vol. 52,p. 1160 - 1163][J.Gen.Chem.USSR (Engl.Transl.),1982,vol. 52,p. 1318 - 1322]
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