Propyl propionate synthesis
- Product Name:Propyl propionate
- CAS Number:106-36-5
- Molecular formula:C6H12O2
- Molecular Weight:116.16
123-38-6
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106-36-5
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Yield:106-36-5 99%
Reaction Conditions:
with [{(PhN)MeC(Nt-Bu)}AlMe(μ-OMe)]2 at 20; for 0.5 h;Inert atmosphere;Schlenk technique;Green chemistry;Tishchenko-Claisen Dismutation;
Steps:
2.5 General procedure employed for the Tishchenko reaction
General procedure: The pre-catalyst, amidinatoaluminum compound (0.8 mmol) was placed in a dry Schlenk flask under a nitrogen atmosphere, and freshly distilled aldehyde (80 mmol) was introduced. The mixture was immediately stirred at room temperature for 30 min to produce the corresponding ester. The reaction was quenched with 0.5 ml of water and the product was distilled to collect the corresponding ester. The yields reported are the isolated yield.
References:
Zhang, Shaofeng;Han, Hongfei;Guo, Zhiqiang;Tong, Hongbo;Wei, Xuehong [Polyhedron,2015,vol. 90,p. 118 - 122]
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