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ChemicalBook CAS DataBase List TETRACHLOROCATECHOL
1198-55-6

TETRACHLOROCATECHOL synthesis

7synthesis methods
-

Yield:-

Reaction Conditions:

with γ-iron(III) oxide;oxalic acid in water; pH=5 at 30;UV-irradiation;pH-value;

Steps:

2.2. Photochemical and adsorption experiments
The stock solution of aqueous PCP (0.075 mM) was prepared as previously reported [2]. In photochemical experiments, the initial PCP concentration was 0.0375 mM with the dosage of 0.4 g L-1 of γ-Fe2O3 and the reaction temperature was performed at 30 °C in all photodegradation experiments. The NaOH or HClO4 was used to adjust the initial pH of suspensions. The photochemical reactor system and the procedure of photochemical experiments were described in detail previously [3]. An 8 W LZC-UV lamp (Luzchem Research, Inc.) with the main emission at 350 nm and a light intensity of 1.2 mW cm-2 was used as a UV light source. Samples were withdrawn at specific time intervals and analyzed immediately after centrifugation at 4500 rpm for 25 min.

References:

Lan, Qing;Cao, Meiyuan;Ye, Zhijun;Zhu, Jishu;Chen, Manjia;Chen, Xuequan;Liu, Chengshuai [Journal of Photochemistry and Photobiology A: Chemistry,2016,vol. 328,p. 198 - 206]

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