Thymine synthesis
- Product Name:Thymine
- CAS Number:65-71-4
- Molecular formula:C5H6N2O2
- Molecular Weight:126.11
Yield:65-71-4 87%
Reaction Conditions:
with acetic acid at 120;
Steps:
20.1 (1) Synthesis of compound 20-2:
To the reactor was added pyrimidine-2,4-dione 20-1 (0.112 g, 1 mmol)Dicumyl peroxide (0.81 g, 3 mmol) and 2 ml of acetic acid,Reaction at 120 ° C, TLC followed the reaction.The crude product obtained after concentration was purified by column chromatography (petroleum ether: ethyl acetate = 1: 1)And purified to give the title product 20-2 (yield 87%)
References:
CN106496130,2017,A Location in patent:Paragraph 0039
139924-84-8
1 suppliers
inquiry
65-71-4
536 suppliers
$5.00/5g
554-01-8
215 suppliers
$9.00/1g
65-71-4
536 suppliers
$5.00/5g