Tribenzylamine synthesis
- Product Name:Tribenzylamine
- CAS Number:620-40-6
- Molecular formula:C21H21N
- Molecular Weight:287.4
100-39-0
432 suppliers
$10.00/10 g
620-40-6
218 suppliers
$7.00/25g
Yield:620-40-6 95%
Reaction Conditions:
with 5-methyl-1,3,4-thiadiazol-2-amine;potassium hydroxide in ethanol;water at 25; for 1 h;
Steps:
Typical experimental procedure for tertiary amines synthesis
General procedure: A mixture of alkyl halide (1.0 mmol) and 5-methyl-1,3,4-thiadiazole-2-amine (1) (0.3 mmol) were added to a flask containing 3 mmol KOH and 2 cm3 EtOH/H2O (10:1). The reaction continued at room temperature under atmospheric conditions until 1 h. The reaction progress was controlled by thin-layer chromatography. The solvent was evaporated under vacuum. Then, crude reaction mixture was purifiedby column chromatography (petroleum ether/ethyl acetate8:1) to give the tertiary amines in good yields.
References:
Soleiman-Beigi, Mohammad;Mohammadi, Fariba [Monatshefte fur Chemie,2017,vol. 148,# 12,p. 2123 - 2128]
100-44-7
642 suppliers
$13.50/250G
620-40-6
218 suppliers
$7.00/25g
100-51-6
1422 suppliers
$5.00/100g
620-40-6
218 suppliers
$7.00/25g
100-46-9
489 suppliers
$5.00/5 g
100-51-6
1422 suppliers
$5.00/100g
620-40-6
218 suppliers
$7.00/25g