1-Bromo-2,6-difluorobenzene synthesis
- Product Name:1-Bromo-2,6-difluorobenzene
- CAS Number:64248-56-2
- Molecular formula:C6H3BrF2
- Molecular Weight:192.99
385-00-2
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64248-56-2
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Yield:64248-56-2 98 %Spectr.
Reaction Conditions:
Stage #1: 2,6-difluorobenzoic acidwith (tri-tert-butylphosphane)gold(I) chloride;silver(l) oxide in N,N-dimethyl-formamide at 100; for 3 h;Inert atmosphere;
Stage #2: with N-Bromosuccinimide in N,N-dimethyl-formamide at 50; for 1 h;Inert atmosphere;
References:
Cornella, Josep;Rosillo-Lopez, Martin;Larrosa, Igor [Advanced Synthesis and Catalysis,2011,vol. 353,# 8,p. 1359 - 1366] Location in patent:supporting information; experimental part
372-18-9
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64248-56-2
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$6.00/1g
5509-65-9
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64248-56-2
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133117-48-3
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64248-56-2
282 suppliers
$6.00/1g