2-Ethylhexyl 4-dimethylaminobenzoate synthesis
- Product Name:2-Ethylhexyl 4-dimethylaminobenzoate
- CAS Number:21245-02-3
- Molecular formula:C17H27NO2
- Molecular Weight:277.4
Take p-dimethylaminobenzaldehyde 149g (1mol) dissolved in 600mL of toluene, keep the system temperature at 5 to 10℃, then add 6.5g KH2PO4 and 100mL of water, stirring dropwise addition of NaClO2 (1.35mol, 122.2g) and 1,000mL prepared aqueous s
104-76-7
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10287-53-3
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21245-02-3
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$34.29/100ml
Yield:21245-02-3 98%
Reaction Conditions:
Stage #1:2-Ethylhexyl alcohol;ethyl p-dimethyaminolbenzoate in xylene for 0.233333 h;Heating;
Stage #2: with TiO(acac)2 in xylene for 30 h;Heating;
References:
Chen, Chien-Tien;Kuo, Jen-Huang;Ku, Cheng-Hsiu;Weng, Shiue-Shien;Liu, Cheng-Yuan [Journal of Organic Chemistry,2005,vol. 70,# 4,p. 1328 - 1339]