2-METHYL-2-OXAZOLINE synthesis
- Product Name:2-METHYL-2-OXAZOLINE
- CAS Number:1120-64-5
- Molecular formula:C4H7NO
- Molecular Weight:85.1
126-33-0
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$5.00/25g
7355-58-0
149 suppliers
$75.00/1g
1120-64-5
156 suppliers
$10.00/1g
Yield:1120-64-5 73%
Steps:
1 EXAMPLE 1
EXAMPLE 1 Preparation of 2-methyl-1,3-oxazoline was as follows. To 10 milliliters (ml) of tetramethylene sulfone (Sulfolane) was added N-(2-chloroethyl) acetamide (2 grams (g), 16 millimoles (mmole)) and 4 equivalents (10 g) of 40% potassium fluoride on alumina. This mixture was mechanically stirred for about two hours. The product was then distilled at 90° C under a vacuum of 550 mm Hg to give 1.018 g (a yield of about 73 percent).
References:
US5382665,1995,A
7355-58-0
149 suppliers
$75.00/1g
1120-64-5
156 suppliers
$10.00/1g
141-43-5
944 suppliers
$9.00/10g
141-78-6
748 suppliers
$22.37/250ml
1120-64-5
156 suppliers
$10.00/1g
142-26-7
184 suppliers
$7.00/5g
1120-64-5
156 suppliers
$10.00/1g