1-(3-Dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride synthesis
- Product Name:1-(3-Dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride
- CAS Number:25952-53-8
- Molecular formula:C8H18ClN3
- Molecular Weight:191.7
1892-57-5
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$5.00/1g
25952-53-8
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$9.00/25g
Yield:25952-53-8 92%
Reaction Conditions:
with triethylamine hydrochloride in acetonitrile at 15; for 1 h;Temperature;
Steps:
Add 1100 g of triethylamine hydrochloride to a 3000 ml reaction flask.1000g of acetonitrile, wherein the mass ratio of triethylamine to HCL is 5:1,EDC213.6g was slowly added dropwise, and the temperature was controlled at 15 °C.The dropping time is controlled at 60 min, filtered,EDC hydrochloride was obtained with a purity of 99.5% and a yield of 92%.
References:
CN109369458,2019,A Location in patent:Paragraph 0025; 0034; 0035; 0039; 0040; 0044
628-13-7
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1892-57-5
321 suppliers
$5.00/1g
25952-53-8
847 suppliers
$9.00/25g
![[3-(Dimethylamino)propyl]dithiocarbamic acid](/CAS/GIF/18997-72-3.gif)
18997-72-3
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25952-53-8
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27421-70-1
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$265.00/250mg
25952-53-8
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109-55-7
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$14.00/25mL
25952-53-8
847 suppliers
$9.00/25g