3-BROMO-N-HYDROXY-BENZAMIDINE synthesis
- Product Name:3-BROMO-N-HYDROXY-BENZAMIDINE
- CAS Number:173406-70-7
- Molecular formula:C7H7BrN2O
- Molecular Weight:215.05
6952-59-6
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$9.00/10g
173406-70-7
39 suppliers
$55.00/250mg
Yield:173406-70-7 100%
Reaction Conditions:
with hydroxylamine hydrate in ethanol at 90; for 1 h;Sealed tube;
Steps:
4.1.4. General procedure for the synthesis of amidoximes (39e52)
General procedure: In a pressurized sealed vial, aqueous hydroxylamine 50% w/w (4equiv) was added to a stirred solution of the appropriate carbonitrile(1 equiv) in absolute ethanol. The resulting mixture washeated at 90 C for 1 h. The solvent was then evaporated to drynessproviding the desired amidoxime quantitatively, which was usedwithout further purification.
References:
Quadri, Marta;Silnovi?, Almin;Matera, Carlo;Horenstein, Nicole A.;Stokes, Clare;De Amici, Marco;Papke, Roger L.;Dallanoce, Clelia [European Journal of Medicinal Chemistry,2018,vol. 160,p. 207 - 228]
3132-99-8
513 suppliers
$5.00/10g
173406-70-7
39 suppliers
$55.00/250mg