4-(Methylphenyl)sulfonylacetonitrile synthesis
- Product Name:4-(Methylphenyl)sulfonylacetonitrile
- CAS Number:5697-44-9
- Molecular formula:C9H9NO2S
- Molecular Weight:195.24
1576-35-8
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5697-44-9
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Yield:5697-44-9 86%
Reaction Conditions:
with dipotassium peroxodisulfate at 80; for 5 h;Temperature;
Steps:
2
In a clean and dry 100 ml round bottom flask, 10 mmol of p-toluenesulfonylhydrazine, 30 mmol of potassium persulfate, 25 ml of acetonitrile were successively added, followed by further reaction at 80 ° C for 5 hours.After the reaction, the reaction solvent was directly dried by a rotary evaporator, and the residue was recrystallized from petroleum ether and dichloromethane.A yellow solid was obtained with a yield of about 86%.
References:
Xinyang Normal University;Tan Meirong CN108558717, 2018, A Location in patent:Paragraph 0033; 0035-0036; 0039
107-14-2
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5697-44-9
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32253-83-1
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![2-[(4-METHYLPHENYL)THIO]ACETONITRILE](/CAS/GIF/21681-88-9.gif)
21681-88-9
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5697-44-9
144 suppliers
$15.00/1g