Ethyl methyl carbonate synthesis
- Product Name:Ethyl methyl carbonate
- CAS Number:623-53-0
- Molecular formula:C4H8O3
- Molecular Weight:104.1
616-38-6
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105-58-8
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623-53-0
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$44.79/10ml
Yield:623-53-0 83.39%
Reaction Conditions:
with Zeolitic imidazole framework (ZIF)-67 at 100; for 24 h;Reagent/catalyst;Concentration;
Steps:
2.3.1 Typical procedure for the synthesis of EMC
A mixture of DMC (9.000g, 0.1mol), DEC (11.800g, 0.1mol) and catalyst (0.200g, 2wt.%), was charged into a 50mL flask equipped with a magnetic stirring and a reflux condenser. The reaction mixture was then heated to 100°C with continuous stirring. After 24h, the mixture was cooled to room temperature. And the product was filtered and analyzed by a gas chromatograph (GC, Agilent-7890A) equipped with a flame-ionized detector. In the reusability experiment, catalysts were separated by filtration and washed using methanol (10mL×3), then dried in air at 150°C for the next reaction.
References:
Yang, Lili;Yu, Lin;Sun, Ming;Gao, Cheng [Catalysis Communications,2014,vol. 54,p. 86 - 90]
64-17-5
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623-53-0
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$44.79/10ml
64-17-5
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124-38-9
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74-88-4
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623-53-0
335 suppliers
$44.79/10ml
64-17-5
897 suppliers
$10.00/50g
616-38-6
725 suppliers
$5.00/5 g
623-53-0
335 suppliers
$44.79/10ml
105-58-8
486 suppliers
$14.00/25g
67-56-1
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74-96-4
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124-38-9
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623-53-0
335 suppliers
$44.79/10ml