Isovaleric acid synthesis
- Product Name:Isovaleric acid
- CAS Number:503-74-2
- Molecular formula:C5H10O2
- Molecular Weight:102.13
590-86-3
382 suppliers
$10.00/5g
503-74-2
454 suppliers
$5.00/10g
Yield:503-74-2 99.1%
Reaction Conditions:
with potassium acetate;palladium diacetate;C34H36O8 at 30 - 35; for 6 h;Catalytic behavior;Inert atmosphere;Reagent/catalyst;
Steps:
7-12 Example 7
General procedure: To a dry 1L three-neck flask, add isovaleraldehyde (160g, 1.86mol), isovaleric acid (160g, 1.57mol), the above ligand L2 (24.8mg, 0.04mmol), palladium acetate (44.9mg, 0.2mmol) ) And potassium acetate 260mg; mechanically stirred under a nitrogen atmosphere, after the temperature rises to 30°C, start to pass in air at a flow rate of 19.8g/h, and keep the reaction temperature between 3035°C by adding cooling water to the water bath Reaction in any range, after 8h reaction, isovaleric acid is prepared.
References:
CN110776412,2020,A Location in patent:Paragraph 0087-0111
123-51-3
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503-74-2
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$5.00/10g
110-62-3
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590-86-3
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503-74-2
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$5.00/10g
109-52-4
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541-47-9
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503-74-2
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123-51-3
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503-74-2
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$5.00/10g
659-70-1
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